| Column: Beksich-Pur ODS-3 and 5um(125 x 4 mm), 流速: 0,5 ml/min. 流动相 A: 20 mM硫酸氢钾/乙腈 (82/18) B: 20 mM硫酸二氢钾/乙腈 (60/40) 梯度: 0-100 % in 30 mins., then at 100 B % Sample: 1= Scoplamine/东莨菪碱 2= Atropine Sulfate/硫酸阿托品 3= Quinine/奎宁;金鸡纳碱 4= Sparteine Sulfate/硫酸金雀花碱 5= Cinchonine/辛可宁 6= Papaverine/ 7= Narcotine/那可汀 |